Propionic Acid → Palladium(II) propionate

HRID 1644135Notes

Reaction equation

HRID 1644135 reaction equation
CC(O)=O.CC(O)=O.[Pd:9].[C:10]([OH:14])(=[O:13])[CH2:11][CH3:12]>>[C:10]([O-:14])(=[O:13])[CH2:11][CH3:12].[Pd+2:9].[C:10]([O-:14])(=[O:13])[CH2:11][CH3:12]

Participants

3

Reactant 2

HCID 1032Propionic AcidHCID 4144353Palladium (II) acetate

Product 1

HCID 11459426Palladium(II) propionate

Procedure

5 gm commercial palladium(II) acetate trimer (Aldrich) was added to 40 g of propionic acid. The mixture was maintained at 40 degrees Celsius for 24 hours. Excess propionic acid was removed under vacuum at room temperature. The resulting yellow solid was used for making palladium inks.

Workup

  1. temperatureThe mixture was maintained at 40 degrees Celsius for 24 hours
  2. customExcess propionic acid was removed under vacuum at room temperature

Sources & evidence

ORD record
ord-4fd46f75baac4cf0b3ee73ef80cf57f0
Source dataset
uspto-grants-2012_02
Patent number
US08124226B2

Reaction notes

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