HRID1644328

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID13204952

6-Methoxy-2H-1,4-benzoxazin-3(4H)-one

C9H9NO3

HCID13690743

未命名化合物

2 次

PRODUCTS

生成物

HCID11788809

未命名化合物

PROCEDURE

实验过程

Prepared from ethyl[(4-methoxy-2-nitrophenyl)thio]acetate (Intermediate 53, 3 g, 11 mmol) according to procedure described for preparation of Intermediate 48. Silica gel chromatography with hexanes/ethyl acetate (3:2) afforded desired product, 2 g (93%).