3,5-Dihydroxybenzoic Acid → HCID 58948855, compound

HRID 1644612Notes

Reaction equation

HRID 1644612 reaction equation
[F:1][C:2]1[CH:18]=[CH:17][CH:16]=[CH:15][C:3]=1[CH2:4][O:5][C:6]1[CH:7]=[C:8]([CH:11]=[C:12]([OH:14])[CH:13]=1)[CH:9]=[O:10].[OH:19][C:20]1C=C(C=C(O)C=1)C(O)=O>>[F:1][C:2]1[CH:18]=[CH:17][CH:16]=[CH:15][C:3]=1[CH2:4][O:5][C:6]1[CH:7]=[C:8]([CH:11]=[C:12]([OH:14])[CH:13]=1)[C:9]([O:19][CH3:20])=[O:10]

Participants

3

Reactant 2

HCID 74243,5-Dihydroxybenzoic AcidHCID 59243097HCID 59243097, compound

Product 1

HCID 58948855HCID 58948855, compound

Procedure

The same experimental conditions were used as described previously for the synthesis of 3-(2-fluorobenzyloxy)-5-hydroxybenzaldehyde (217a) except that the reaction began with 3,5-dihydroxy benzoic acid. The LC/MS gave a calculated and found (M+H+)=277.

Workup

  1. customThe LC/MS gave a calculated and

Sources & evidence

ORD record
ord-4ebd1212c92546bd9325229b419ec221
Source dataset
uspto-grants-2012_02
Patent number
US08124617B2

Reaction notes

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