HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Nitrobenzenesulfonyl chloride → HCID 59152956, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Nitrobenzenesulfonyl chloride | HCID 8476 | — |
| Reactant | HCID 59152911 | HCID 59152911 | — |
| Product | HCID 59152956 | HCID 59152956 | 63.6% |
Reaction Steps
Starting with (4-amino-4,5,6,7-tetrahydro-indazol-1-yl)-acetic acid ethyl ester and 3-nitro-benzenesulfonyl chloride using the method analogous to the one described above for example 1-1, [4-(3-nitro-benzenesulfonylamino)-4,5,6,7-tetrahydro-indazol-1-yl]-acetic acid ethyl ester (519 mg, 63.6%) was obtained as a white solid. MS cald. for C17H20N4O6S 408, obsd. (ESI+) [(M+H)+] 409.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08124641B2 |
| Source dataset | uspto-grants-2012_02 |
| ORD ID | ord-c884f947c6b54909b581e10a0d227afb |
| Source note | uspto-grants-2012_02 |