O-Phenylenediamine → HCID 66775704, compound

HRID 1645202Notes

Reaction equation

HRID 1645202 reaction equation
[NH:1]1[C@H:6]([C:7]([O-])=O)[CH2:5][CH2:4][CH2:3][C@@H:2]1[C:10]([O-])=O.[C:13]1([NH2:20])[CH:18]=[CH:17][CH:16]=[CH:15][C:14]=1[NH2:19]>>[NH:19]1[C:14]2[CH:15]=[CH:16][CH:17]=[CH:18][C:13]=2[N:20]=[C:7]1[C@H:6]1[NH:1][C@@H:2]([C:10]2[NH:20][C:13]3[CH:18]=[CH:17][CH:16]=[CH:15][C:14]=3[N:19]=2)[CH2:3][CH2:4][CH2:5]1

Participants

3

Reactant 2

HCID 7243O-PhenylenediamineHCID 131729475HCID 131729475, compound

Product 1

HCID 66775704HCID 66775704, compound

Procedure

2k was synthesised by an analogous procedure to that described for 2a using cis-2,6-piperidinedicarboxilate (1.4 g, 6.97 mmol) and o-phenylenediamine (1.51 g, 13.94). Yield 1.92 g (87%).

Sources & evidence

ORD record
ord-d016f880687445e991ed4bd5b55e29ad
Source dataset
uspto-grants-2012_02
Patent number
US08124698B2

Reaction notes

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