HuagongsheHuagongshe Chemistry Print Report · For research reference only
N,N-bis(1H-benzimidazol-2-ylmethyl)-N-benzylamine chromium (III) chloride → HCID 86638470, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N,N-bis(1H-benzimidazol-2-ylmethyl)-N-benzylamine chromium (III) chloride | HCID 86638462 | — |
| Reactant | N,N-bis(1H-benzimidazol-2-ylmethyl)amine chromium (III) chloride hexafluoroantimonate tetrahydrofuran | HCID 86638469 | — |
| Catalyst | Silver hexafluoroantimonate | HCID 16687962 | — |
| Product | HCID 86638470 | HCID 86638470 | — |
Reaction Steps
4d was synthesised by an analogous procedure to that described for 4a using silver hexafluoroantimonate (0.20 g, 0.57 mmol) and complex 3d (0.30 g, 0.57 mmol). Yield 0.31 g, 68%. +FAB-MS: (m/e): 489 ([M]+), 454 ([M-Cl]+). −FAB-MS: (m/z): 235 ([M]−).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08124698B2 |
| Source dataset | uspto-grants-2012_02 |
| ORD ID | ord-a1b2b7bf60704172a50648da50812bc5 |
| Source note | uspto-grants-2012_02 |