HCID 66775446, compound → HCID 58807411, compound

HRID 1645454Notes

Reaction equation

HRID 1645454 reaction equation
[Br:1][C:2]1[CH:3]=[C:4]([F:15])[C:5]([CH:9]=[CH:10][C@H:11]([CH3:14])[CH2:12][CH3:13])=[C:6]([F:8])[CH:7]=1>CCCCCCC>[Br:1][C:2]1[CH:7]=[C:6]([F:8])[C:5]([CH2:9][CH2:10][C@H:11]([CH3:14])[CH2:12][CH3:13])=[C:4]([F:15])[CH:3]=1

Participants

3

Reactant 1

HCID 66775446HCID 66775446, compound

Product 1

HCID 58807411HCID 58807411, compound

Reagents, catalysts & solvents 1

HCID 8900HeptaneSolvent

Procedure

0.4 g of 5% PVC (dry) is added to a solution of 1.8 g (5.9 mmol) of 2 in 0.50 ml of heptane, and the mixture is hydrogenated at atmospheric pressure for 20 hours. The solvent is removed under reduced pressure, and the entire amount is converted into 4,

Workup

  1. customThe solvent is removed under reduced pressure

Sources & evidence

ORD record
ord-780fef6eafd643bb9943db182af63443
Source dataset
uspto-grants-2012_02
Patent number
US08124817B2

Reaction notes

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