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HRID1645485

反应详情

EQUATION

反应方程式

HRID 1645485 的结构方程式

REACTANTS

反应物

2
反应SMILES：O=S(Cl)Cl
HCID24386

Thionyl chloride

Cl2OS

反应SMILES：CC(=O)OCC(OC(C)=O)C(OC(C)=O)C(=O)O
HCID77215762

未命名化合物

PRODUCTS

产物

1
反应SMILES：CC(=O)OCC(OC(C)=O)C(OC(C)=O)C(=O)Cl
HCID18429135

未命名化合物

PROCEDURE

实验过程

The 2,3,4-triacetoxy-butyric acid (25 g, 0.095 mol) was stirred in thionyl chloride (15.3 mL) at room temperature with a condenser fitted. The reaction was stirred for 48 hours and then the thionyl chloride was removed under reduced pressure to give an oil, which 1H and 13C NMR (CDCl3) showed to be the desired material (26.1 g, 98%).

WORKUP

后处理

  1. customfitted
  2. customthe thionyl chloride was removed under reduced pressure
  3. customto give an oil, which 1H and 13C NMR (CDCl3)