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HRID1645606

反应详情

EQUATION

反应方程式

HRID 1645606 的结构方程式

REACTANTS

反应物

3
结构：Cc1c(Cl)cc[n+]([O-])c1C
HCID9877446

4-Chloro-2,3-dimethyl-1-oxo-1lambda~5~-pyridine

C7H8ClNO

结构：CCC1(CO)OCCCO1
HCID59792489

未命名化合物

结构：CCCC1(CCOc2ccnc(CS(=O)c3nc4ccccc4[nH]3)c2C)OCCO1.[Na]
HCID66775818

未命名化合物

PRODUCTS

生成物

1
结构：CCC1(COc2ccnc(CS(=O)c3nc4ccccc4[nH]3)c2C)OCCCO1.[Na]
HCID66776228

未命名化合物

收率 9.6%

PROCEDURE

实验过程

The same procedure as in the steps (3c) to (3h) of Example 3 was repeated using 4-chloro-2,3-dimethylpyridine 1-oxide and (2-ethyl-1,3-dioxan-2-yl)methanol to obtain the title compound (305 mg, 6 steps: 9.6%) as a solid.