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HRID1645617

反应详情

EQUATION

反应方程式

HRID 1645617 的结构方程式

REACTANTS

反应物

3
结构：Cc1c(Cl)cc[n+]([O-])c1C
HCID9877446

4-Chloro-2,3-dimethyl-1-oxo-1lambda~5~-pyridine

C7H8ClNO

结构：OCC1OCC(F)(F)CO1
HCID59792439

未命名化合物

结构：Cc1c(OCC2OCC(C)(C)CO2)ccnc1CS(=O)c1nc2ccccc2[nH]1.[Na]
HCID66776588

未命名化合物

PRODUCTS

生成物

1
结构：Cc1c(OCC2OCC(F)(F)CO2)ccnc1CS(=O)c1nc2ccccc2[nH]1.[Na]
HCID66776087

未命名化合物

收率 22.7%

PROCEDURE

实验过程

The same procedure as in the steps (1c) to (1g) of Example 1 was repeated using 4-chloro-2,3-dimethylpyridine 1-oxide and (5,5-difluoro-1,3-dioxan-2-yl)methanol to obtain the title compound (375 mg, 5 steps: 22.7%) as a white powder.