HuagongsheHuagongshe Chemistry Print Report · For research reference only
Fumaric Acid → HCID 19390835, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Fumaric Acid | HCID 444972 | — |
| Reactant | HCID 19390836 | HCID 19390836 | — |
| Product | HCID 19390835 | HCID 19390835 | 95.5% |
Reaction Steps
The 1-benzyl-4-[4-(4-pyrrolidinobenzoyl)butyl]piperidine (0.5 g) prepared in 5) was treated with one equivalent of fumaric acid (0.14 g) and the reaction product was crystallized from ethanol to give 0.6 g of 1-benzyl-4-[4-(4-pyrrolidinobenzoyl)butyl]piperidine fumarate as colorless crystals melting at 183°-185° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05177087 |
| Source dataset | uspto-grants-1993_01 |
| ORD ID | ord-0acbd4b73e4045239f1b4d0e2d5c22c1 |
| Source note | uspto-grants-1993_01 |