HRID1645996

反应详情

EQUATION

反应方程式

HRID 1645996 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

18.5 g (0.1 mol) of ethyl N-allyl-N-(1-oxoprop-2-yl)-carbamate are heated under reflux overnight in a water separator with 9 g (0.1 mol) of sarcosine in 300 ml of toluene. The mixture is concentrated and the residue is distilled.

WORKUP

后处理

  1. concentrationThe mixture is concentrated
  2. distillationthe residue is distilled