HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → HCID 19100936, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | 2-(Benzylamino)acetic acid | HCID 86965 | — |
| Reactant | Ethyl N-allyl-N-(1-oxoprop-2-yl)-carbamate | HCID 15069993 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 19100936 | HCID 19100936 | — |
Reaction Steps
37 g (0.2 mol) of ethyl N-allyl-N-(1-oxo-2-propyl)-carbamate are heated under reflux overnight in a water separator with 33 g (0.2 mol) of N-benzylglycine in 500 ml of toluene. The mixture is concentrated and the residue is distilled.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05177210 |
| Source dataset | uspto-grants-1993_01 |
| ORD ID | ord-3ac9ea861bf843848a0cc3d3d9204736 |
| Source note | uspto-grants-1993_01 |