HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → HCID 19100948, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | Toluene | HCID 1140 | — |
| Reactant | 2-(Benzylamino)acetic acid | HCID 86965 | — |
| Reactant | ethyl N-(but-2-enyl)-N-(2-oxoethyl)-carbamate | HCID 53690408 | — |
| Product | HCID 19100948 | HCID 19100948 | — |
Reaction Steps
18.5 g (0.1 mol) of ethyl N-(2-buten-1-yl)-N-(2-oxoethyl)-carbamate are heated under reflux overnight in a water separator with 16.5 g (0.1 mol) of N-benzylglycine in 300 ml of toluene. The mixture is concentrated and the residue is distilled.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05177210 |
| Source dataset | uspto-grants-1993_01 |
| ORD ID | ord-a3e0a57bb02c44a9a138015fe7200411 |
| Source note | uspto-grants-1993_01 |