HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 19100950, compound → HCID 19100969, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 19100950 | HCID 19100950 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 19100969 | HCID 19100969 | — |
Reaction Steps
13 g (44.9 mmol) of ethyl 2-benzyl-6-methyl-2,7-diazabicyclo[3.3.0]octane-7-carboxylate in 150 ml of ethanol are hydrogenated ar 100° C. and 100 bar on 2 g of palladium-active carbon (10% Pd). The catalyst is filtered off, the filtrate is concentrated and the residue is distilled.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05177210 |
| Source dataset | uspto-grants-1993_01 |
| ORD ID | ord-5c8bf74d9ed84c2a88c720538d27931f |
| Source note | uspto-grants-1993_01 |