HCID 53729649, compound → HCID 54097825, compound

Participants

Reaction Steps

Under one atmosphere, a solution of 300 mg of 5-[3-(4-chlorophenylsulfonyl)-1-propenyl]-2-methoxymethoxy nitrobenzene in 8 ml of ethyl acetate and 500 mg of 10% palladium carbon added thereto were stirred in the presence of hydrogen gas. The resultant reaction mixture was filtered and then concentrated under a vacuum, to produce 220 mg of 5-[3-(4-chlorobenzenesulfonyl)propyl]-2-methoxymethoxy aniline in the form of a colorless oily substance. The yield was 73%. This product was put to use in its unpurified form in the following reaction.

Provenance & Evidence