2-[(Acetylthio)methyl]-3-phenylpropionic Acid → HCID 15670219, compound

HRID 1646303Notes

Reaction equation

HRID 1646303 reaction equation
[NH2:1][C:2]1([C:8]([O:10][CH2:11][C:12]2[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=2)=[O:9])[CH2:7][CH2:6][CH2:5][CH2:4][CH2:3]1.C1(C)C=CC(S([O-])(=O)=O)=CC=1.[C:29]([S:32][CH2:33][CH:34]([CH2:38][C:39]1[CH:44]=[CH:43][CH:42]=[CH:41][CH:40]=1)[C:35](O)=[O:36])(=[O:31])[CH3:30]>>[C:29]([S:32][CH2:33][CH:34]([CH2:38][C:39]1[CH:40]=[CH:41][CH:42]=[CH:43][CH:44]=1)[C:35]([NH:1][C:2]1([C:8]([O:10][CH2:11][C:12]2[CH:13]=[CH:14][CH:15]=[CH:16][CH:17]=2)=[O:9])[CH2:7][CH2:6][CH2:5][CH2:4][CH2:3]1)=[O:36])(=[O:31])[CH3:30]

Participants

3

Reactant 2

HCID 99917962-[(Acetylthio)methyl]-3-phenylpropionic AcidHCID 86746490HCID 86746490, compound

Product 1

HCID 15670219HCID 15670219, compound

Procedure

Benzyl 1-aminocyclohexanecarboxylate·p-toluene-sulfonate and 2-acetylthiomethyl-3-phenylpropionic acid are reacted in the same manner as described in Example 68-(a)-[1] to give the title compound.

Sources & evidence

ORD record
ord-97a5e1d5bbce419a9889d15da6882a60
Source dataset
uspto-grants-1993_01
Patent number
US05179125

Reaction notes

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