HuagongsheHuagongshe Chemistry Print Report · For research reference only
Butyl chloroformate → Methyl 4-[6-(butoxycarbonyl)aminobenzimidazol-1-ylmethyl]-3-methoxybenzoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Butyl chloroformate | HCID 61140 | — |
| Reactant | Methyl 4-(6-aminobenzimidazol-1-ylmethyl)-3-methoxybenzoate | HCID 14763098 | — |
| Product | Methyl 4-[6-(butoxycarbonyl)aminobenzimidazol-1-ylmethyl]-3-methoxybenzoate | HCID 23365847 | 34% |
Reaction Steps
Using a similar procedure to that described in Example 35, but using butyl chloroformate and (J), the title compound was obtained as a solid in 34% yield; partial NMR: 0.9 (t,3 H, CH3CH2), 1.4 (m,2 H, CH3CH2), 1.6 (m,2 H, CH2CH2O), 4.1 (t,2 H, CH2O).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05179112 |
| Source dataset | uspto-grants-1993_01 |
| ORD ID | ord-a2b76f9a9c6d4e20b4ffdc0c7d3e7245 |
| Source note | uspto-grants-1993_01 |