HuagongsheHuagongshe Chemistry Print Report · For research reference only
p-Toluenesulfonic acid → HCID 21218303, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | p-Toluenesulfonic acid | HCID 6101 | — |
| Reactant | Trimethyl orthoformate | HCID 9005 | — |
| Reactant | 2,3-Dimethyl-5-nitroaniline | HCID 820786 | — |
| Product | HCID 21218303 | HCID 21218303 | — |
Reaction Steps
66.4 g of 2,3-dimethyl-5-nitroaniline, 0.4 liter of trimethyl orthoformate and 1.6 g of paratoluenesulphonic acid are mixed and the mixture is refluxed for 3 hours.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05180400 |
| Source dataset | uspto-grants-1993_01 |
| ORD ID | ord-7f0728382f4e47b5ac7a904965900667 |
| Source note | uspto-grants-1993_01 |