HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 19800639, compound → HCID 85650396, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 19800639 | HCID 19800639 | — |
| Reactant | HCID 19800664 | HCID 19800664 | — |
| Solvent | Sulfuric Acid | HCID 1118 | — |
| Solvent | Acetic Anhydride | HCID 7918 | — |
| Product | HCID 85650396 | HCID 85650396 | — |
Reaction Conditions
| Temperature | 110 °C |
|---|
Reaction Steps
A 4:1 mixture of 3-acetamido-4-hydroxyphthalic acid and 2-methyl-4,5-benzoxazoledicarboxylic acid in acetic anhydride and concentrated sulfuric acid (0.10 mL) is stirred for 18 hours at 110° C., cooled and filtered. The white solid filter cake is air dried to give the title product, 5.39 g (77.1%), identified by NMR and IR spectral analyses.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05180419 |
| Source dataset | uspto-grants-1993_01 |
| ORD ID | ord-4be665be9e454a2799d865382c3b5b68 |
| Source note | uspto-grants-1993_01 |