HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-oxo-2,3-dihydro-1H-indene-5-carbonitrile → 1-hydroxy-2,3-dihydro-1H-indene-5-carbonitrile
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-oxo-2,3-dihydro-1H-indene-5-carbonitrile | HCID 312896 | — |
| Solvent | Hexane | HCID 8058 | — |
| Product | 1-hydroxy-2,3-dihydro-1H-indene-5-carbonitrile | HCID 14515323 | — |
Reaction Steps
The operation is carried out as in preparation 10, starting with 5-cyano-1-indanone (1.93 g), the extracted residue is taken up in 20 ml of hexane, with agitation for one hour. After filtering, the filtrate is dried at 45° C. under reduced pressure and 1.92 g is obtained,
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05180741 |
| Source dataset | uspto-grants-1993_01 |
| ORD ID | ord-2eae400e965f4daf84e7cb16d725c5d4 |
| Source note | uspto-grants-1993_01 |