Dichloromethane → N-vinylbenzyl-N-2-picolylamine

HRID 1646661Notes

Reaction equation

N1C=CC=[CH:3][C:2]=1CN.N1[CH:14]=[CH:13][CH:12]=[CH:11][C:10]=1[CH2:15][NH:16][CH2:17][C:18]1[CH:23]=[CH:22][CH:21]=[CH:20][N:19]=1.[CH2:24](Cl)Cl>>[CH:2]([N:16]([CH2:15][C:10]1[CH:24]=[CH:14][CH:13]=[CH:12][CH:11]=1)[CH2:17][C:18]1[CH:23]=[CH:22][CH:21]=[CH:20][N:19]=1)=[CH2:3]

Participants

Reactant 3

HCID 6344Dichloromethane

HCID 195092-Pyridinemethanamine

HCID 73759Bis(2-pyridylmethyl)amine

Product 1

HCID 67775753N-vinylbenzyl-N-2-picolylamine

Procedure

The procedure described in Example 1 above was carried out with 43.3 g (0.4 mole) of 2-picolylamine substituted for the bis-2-picolylamine. Concentration of the methylene chloride gave 82.5 g of the N-vinylbenzyl-N-2-picolylamine monomer.

Sources & evidence

ORD record: ord-83ab460dc4b44785bfffbf0cb9d20acd
Source dataset: uspto-grants-1993_01
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US05180822

Reaction notes

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