Water → HCID 54427044, compound

HRID 1646686Notes

Reaction equation

HRID 1646686 reaction equation
[OH2:1].[CH:2]([C:4]1[CH:5]=[C:6]([C:10](=[N:17][O:18][CH2:19][CH2:20][CH2:21][CH2:22][C:23]([OH:25])=[O:24])[C:11]2[CH:12]=[N:13][CH:14]=[CH:15][CH:16]=2)[CH:7]=[CH:8][CH:9]=1)=[O:3]>[Ag-]=O.C(O)C>[C:23]([CH2:22][CH2:21][CH2:20][CH2:19][O:18][N:17]=[C:10]([C:11]1[CH:12]=[N:13][CH:14]=[CH:15][CH:16]=1)[C:6]1[CH:5]=[C:4]([CH:9]=[CH:8][CH:7]=1)[C:2]([OH:1])=[O:3])([OH:25])=[O:24]

Participants

5

Reactant 2

HCID 962WaterHCID 54185565HCID 54185565, compound

Product 1

HCID 54427044HCID 54427044, compound

Reagents, catalysts & solvents 2

HCID 178418778HCID 178418778, compoundCatalystHCID 702EthanolSolvent

Procedure

A mixture of 6.5 parts of silver(I) oxide, 50 parts of water, 63 parts of ethanol and 6.5 parts of 5-[[[(3-formylphenyl)(3-pyridinyl)methylen]amino]oxy]pentanoic acid is stirred for 1 hour at a somewhat elevated temperature to give 3-[[(4-carboxybutoxy)imino](3-pyridinyl)methyl]benzoic acid (compound 126).

Sources & evidence

ORD record
ord-b75631ee26e6488a80391f67ebdc3955
Source dataset
uspto-grants-1993_01
Patent number
US05180832

Reaction notes

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