HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 10039421, compound → HCID 9990821, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 10039421 | HCID 10039421 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 9990821 | HCID 9990821 | 9% |
Reaction Steps
A solution of N-[2-(3-ethylindol-2yl)ethyl]-1-imidazolecarboxamide (2.2 g) in toluene (50 ml) was refluxed for 3 hours. After the mixture was evaporated in vacuo, the residue was purified by silica gel column chromatography (5% methanol-chloroform) to give 5-ethyl-3,4-dihydropyrimido[1,6-a]indol-1(2H)-one (0.15 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05180728 |
| Source dataset | uspto-grants-1993_01 |
| ORD ID | ord-1a93b052591f4d0b8ff7fbec3c7fe66d |
| Source note | uspto-grants-1993_01 |