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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1646765Generated: October 31, 2026

HCID 10039421, compound → HCID 9990821, compound

https://huagongshe.com/reaction/1646765

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 10039421HCID 10039421—
SolventTolueneHCID 1140—
ProductHCID 9990821HCID 99908219%

Reaction Steps

A solution of N-[2-(3-ethylindol-2yl)ethyl]-1-imidazolecarboxamide (2.2 g) in toluene (50 ml) was refluxed for 3 hours. After the mixture was evaporated in vacuo, the residue was purified by silica gel column chromatography (5% methanol-chloroform) to give 5-ethyl-3,4-dihydropyrimido[1,6-a]indol-1(2H)-one (0.15 g).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05180728
Source datasetuspto-grants-1993_01
ORD IDord-1a93b052591f4d0b8ff7fbec3c7fe66d
Source noteuspto-grants-1993_01