HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanolamine → HCID 14209237, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanolamine | HCID 700 | — |
| Reactant | 3-Bromo-4-chloro-7-(trifluoromethyl)quinoline | HCID 45599640 | — |
| Solvent | Water | HCID 962 | — |
| Solvent | Isopropanol | HCID 3776 | — |
| Product | HCID 14209237 | HCID 14209237 | — |
Reaction Steps
A solution of 12.4 g of 3-bromo-4-chloro-7-trifluoromethylquinoline and 6.1 g of 2-aminoethanol in 30 ml of isopropanol was heated at reflux for 4 hours. The mixture was cooled and diluted with 150 ml of water and the solid was collected and recrystallized from isopropanol. The yield was 8.2 g, mp 140°-141° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05182275 |
| Source dataset | uspto-grants-1993_01 |
| ORD ID | ord-053509a8deee465aa8a2eb31f9936a0e |
| Source note | uspto-grants-1993_01 |