Epichlorohydrin → HCID 14880475, compound

HRID 1646947Notes

Reaction equation

HRID 1646947 reaction equation
[NH:1]1[C:9]2[C:4](=[C:5]([CH2:10][C:11]3[CH:16]=[CH:15][CH:14]=[CH:13][C:12]=3[OH:17])[CH:6]=[CH:7][CH:8]=2)[CH:3]=[CH:2]1.[CH2:18]([CH:20]1[O:22][CH2:21]1)Cl>>[O:22]1[CH2:21][CH:20]1[CH2:18][O:17][C:12]1[CH:13]=[CH:14][CH:15]=[CH:16][C:11]=1[CH2:10][C:5]1[CH:6]=[CH:7][CH:8]=[C:9]2[C:4]=1[CH:3]=[CH:2][NH:1]2

Participants

3

Reactant 2

HCID 7835EpichlorohydrinHCID 14880474HCID 14880474, compound

Product 1

HCID 14880475HCID 14880475, compound

Procedure

Using the procedure of Step A of Example 2, 10.0 g of the product of Step A and 3 times 17.56 m1 of epichlorhydrin were reacted to obtain 12.5 g of the desired product melting at 78° C. which was used as is for the following step.

Workup

  1. customwere reacted

Sources & evidence

ORD record
ord-05c304a2181e42098dd9027f87e8aa7d
Source dataset
uspto-grants-1993_01
Patent number
US05182282

Reaction notes

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