Ethyl acetate hexane → HCID 86746512, compound

HRID 1646970Notes

Reaction equation

HRID 1646970 reaction equation
[CH3:1][O:2][C:3]1[CH:24]=[CH:23][C:6]([C:7]([C:9]2([CH2:18][C:19]([O:21][CH3:22])=[O:20])[CH2:17][CH:16]=[C:12]3[CH:13]=[CH:14][CH:15]=[C:11]3[O:10]2)=[O:8])=[CH:5][CH:4]=1.[CH2:25]([O:27][C:28](=O)C)C.CCCCCC>>[CH3:25][O:27]/[CH:28]=[C:18](\[C:9]1([C:7](=[O:8])[C:6]2[CH:23]=[CH:24][C:3]([O:2][CH3:1])=[CH:4][CH:5]=2)[CH2:17][CH:16]=[C:12]2[CH:13]=[CH:14][CH:15]=[C:11]2[O:10]1)/[C:19]([O:21][CH3:22])=[O:20]

Participants

3

Reactant 2

HCID 21226206Ethyl acetate hexaneHCID 67875971HCID 67875971, compound

Product 1

HCID 86746512HCID 86746512, compound

Procedure

Using the procedure of Example 1, methyl 2-(4-methoxy-benzoyl) -7-benzofuranacetate, prepared hereafter, was reacted to obtain the desired product with a Rf 0.07 (eluant: hexane - ethyl acetate (75-25)).

Workup

  1. customprepared hereafter
  2. customwas reacted

Sources & evidence

ORD record
ord-779501c8787a4550a9227008a64aaee3
Source dataset
uspto-grants-1993_01
Patent number
US05182295

Reaction notes

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