Benzyl Alcohol → HCID 131717726, compound

HRID 1646998Notes

Reaction equation

HRID 1646998 reaction equation
[OH:1][C:2]1[CH:7]=[CH:6][C:5]([C:8]([C:11]2[CH:16]=[CH:15][C:14]([OH:17])=[CH:13][CH:12]=2)([CH3:10])[CH3:9])=[CH:4][CH:3]=1.[B:18]([O:35]CC1C=CC=CC=1)([O:27]CC1C=CC=CC=1)[O:19][CH2:20][C:21]1[CH:26]=[CH:25][CH:24]=[CH:23][CH:22]=1.C(O)C1C=CC=CC=1>>[CH2:20]([C:7]1[CH:6]=[C:5]([C:8]([C:11]2[CH:12]=[CH:13][C:14]([OH:17])=[CH:15][CH:16]=2)([CH3:10])[CH3:9])[CH:4]=[CH:3][C:2]=1[OH:1])[C:21]1[CH:26]=[CH:25][CH:24]=[CH:23][CH:22]=1.[B:18]([O-:35])([O-:27])[O-:19]

Participants

4

Reactant 3

HCID 244Benzyl AlcoholHCID 6623Bisphenol AHCID 17179Boric acid, tribenzyl ester

Product 1

HCID 131717726HCID 131717726, compound

Procedure

34g Of bisphenol-A and 100g of tribenzyl borate were stirred under a pressure of 0.5-10mm Hg at a temperature of 120° C. During the reaction benzyl alcohol (28g) was distilled over. The residue was a clear viscous liquid. The compound has a Tg-value below 0° C.

Workup

  1. distillationwas distilled over
  2. customhas a Tg-value below 0° C.

Sources & evidence

ORD record
ord-0757ef8c59d34ea4bdaa5d5481349e73
Source dataset
uspto-grants-1993_01
Patent number
US05182325

Reaction notes

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