Ammonia → HCID 19800400, compound

HRID 1647005Notes

Reaction equation

HRID 1647005 reaction equation
[CH2:1]([O:11][CH2:12][CH:13](Cl)[C:14]([OH:16])=[O:15])[CH2:2][O:3][CH2:4][CH2:5][O:6][CH2:7][CH2:8][O:9][CH3:10].[NH3:18]>>[CH2:1]([O:11][CH2:12][CH:13]([NH2:18])[C:14]([OH:16])=[O:15])[CH2:2][O:3][CH2:4][CH2:5][O:6][CH2:7][CH2:8][O:9][CH3:10]

Participants

3

Reactant 2

HCID 222AmmoniaHCID 19800436HCID 19800436, compound

Product 1

HCID 19800400HCID 19800400, compoundYield 70%

Procedure

This product is obtained with a melting point of 184°-185° C. and a yield of 70% by treatment of 3-(3,6,9-trioxadecyloxy)-2-chloropropionic acid (Ex. 11A) with 25% ammonia (1 mol/3.5 mol) at 115° C. for two hours and removal of the salts by passage through an ion exchange resin column.

Workup

  1. customThis product is obtained with a melting point of 184°-185° C.
  2. customremoval of the salts by passage through an ion exchange resin column

Sources & evidence

ORD record
ord-4819d9065a7149479dd98924394282a2
Source dataset
uspto-grants-1993_01
Patent number
US05182370

Reaction notes

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