N-((1,1-dimethylethoxy)carbonyl)-beta-alanine → HCID 9998006, compound

HRID 1647107Notes

Reaction equation

HRID 1647107 reaction equation
[C:1]([O:5][C:6]([NH:8][CH2:9][CH2:10][C:11]([OH:13])=O)=[O:7])([CH3:4])([CH3:3])[CH3:2].[CH2:14]([O:21][C:22](=[O:26])[CH2:23][CH2:24][NH2:25])[C:15]1[CH:20]=[CH:19][CH:18]=[CH:17][CH:16]=1>>[CH2:14]([O:21][C:22](=[O:26])[CH2:23][CH2:24][NH:25][C:11](=[O:13])[CH2:10][CH2:9][NH:8][C:6]([O:5][C:1]([CH3:2])([CH3:3])[CH3:4])=[O:7])[C:15]1[CH:20]=[CH:19][CH:18]=[CH:17][CH:16]=1

Participants

3

Reactant 2

HCID 76809N-((1,1-dimethylethoxy)carbonyl)-beta-alanineHCID 1116164Benzyl 3-aminopropanoate

Product 1

HCID 9998006HCID 9998006, compound

Procedure

N-(t-butoxycarbonyl)-β-alanine and β-alanine benzyl ester were coupled analogously to the above examples to give N-[N-(t-butoxycarbonyl)-β-alanyl]-β-alanine benzyl ester, mp. 84°-85° C.

Sources & evidence

ORD record
ord-20cb4b885dca4e4fa0ecb3c4e1a30a4e
Source dataset
uspto-grants-1995_07
Patent number
US05430024

Reaction notes

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