HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 131718332, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Methanesulfonamide | HCID 72879 | — |
| Reactant | N-(tert-Butoxycarbonyl)-3-naphthalen-1-yl-D-alanine | HCID 2734502 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 131718332 | HCID 131718332 | 96.8% |
Reaction Steps
Boc-D-1-Nal-OH (0.50 g), methanesulfonamide (0.18 g) DMAP (0.23 g), WSCD.HCl (0.37 g) and CH2Cl2 (10 ml) were reacted in a similar manner to that of Preparation 1-1) to give Boc-D-1-Nal-methanesulfonamide (0.63 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05430022 |
| Source dataset | uspto-grants-1995_07 |
| ORD ID | ord-b0de804f14ea4656815d4965063e360f |
| Source note | uspto-grants-1995_07 |