HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 131718334, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Benzenesulfonamide | HCID 7370 | — |
| Reactant | Boc-D-phenylalanine | HCID 637610 | — |
| Catalyst | 4-(Dimethylamino)pyridine | HCID 14284 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 131718334 | HCID 131718334 | 100.5% |
Reaction Steps
Boc-D-Phe-OH (0.20 g), benzenesulfonamide (0.13 g), DMAP (0.11 g) WSCD.HCl (0.17 g) and CH2Cl2 (4 ml) were reacted in a similar manner to that of Preparation 1-1) to give Boc-D-Phe-benzenesulfonamide (0.32 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05430022 |
| Source dataset | uspto-grants-1995_07 |
| ORD ID | ord-3e34888664b7499a932af28e87852e83 |
| Source note | uspto-grants-1995_07 |