Water → HCID 15294686, compound

HRID 1647191Notes

Reaction equation

HRID 1647191 reaction equation
[NH:1]1C[CH2:4][CH2:3][CH:2]1[CH2:6][S:7]([OH:10])(=[O:9])=[O:8].[OH2:11]>>[NH2:1][CH:2]([CH:3]([OH:11])[CH3:4])[CH2:6][S:7]([OH:10])(=[O:9])=[O:8]

Participants

3

Reactant 2

HCID 962WaterHCID 42882912-Pyrrolidinemethanesulfonic acid2×

Product 1

HCID 15294686HCID 15294686, compound

Procedure

NMR (0.2 NaOD, t-BuOD, δ=1.23 ppm): δ1.17(3H,d,J=6.5 Hz), 2.83(1H,dd,J=9 Hz, 14 Hz), 3.10(1H,dd,J=2.5 Hz, 14 Hz), 3.11-3.17(1H,m), 3.77-3.84(1 H,m) 2-Pyrrolidinylmethanesulfonic acid (compound 23) m.p.: 307°-308° C. (decomposition) [α]24 : +33.4° (c=1.0, H2O) Elementary Analysis: C5H11NO3S

Sources & evidence

ORD record
ord-ae37febe60f44395a95b039ae70773e6
Source dataset
uspto-grants-1995_07
Patent number
US05430052

Reaction notes

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