HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanol → 3-(3-Oxo-3-phenyl-1-propenyl)-benzoic acid, methyl ester
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanol | HCID 887 | — |
| Reactant | 3-(3-Oxo-3-phenyl-1-propenyl)-benzoic acid | HCID 54028671 | — |
| Catalyst | Sulfuric Acid | HCID 1118 | — |
| Product | 3-(3-Oxo-3-phenyl-1-propenyl)-benzoic acid, methyl ester | HCID 86060726 | — |
Reaction Steps
A slurry of 3-(3-oxo-3-phenyl-1-propenyl)-benzoic acid (2.84 g, 11.26 mmol) in methanol (150 mL) is treated with a few drops of sulfuric acid and heated under reflux for 8 hours. Upon cooling, a solid forms which is collected by filtration and washed thoroughly with methanol to provide 0.9 g of the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05430047 |
| Source dataset | uspto-grants-1995_07 |
| ORD ID | ord-01adc58a6aba4a299f8247ba4ee41c3e |
| Source note | uspto-grants-1995_07 |