Isopropylamine → HCID 19926931, compound

HRID 1647277Notes

Reaction equation

HRID 1647277 reaction equation
[C:1]([C:4]1[C:5](=[O:21])[NH:6][C:7]2[C:12]([C:13]=1C)=[C:11](OS(O)(=O)=O)[CH:10]=[CH:9][C:8]=2[CH3:20])(=[O:3])[CH3:2].[CH:22]([NH2:25])([CH3:24])[CH3:23]>>[C:1]([C:4]1[C:5](=[O:21])[NH:6][C:7]2[C:12]([C:13]=1[NH:25][CH:22]([CH3:24])[CH3:23])=[CH:11][CH:10]=[CH:9][C:8]=2[CH3:20])(=[O:3])[CH3:2]

Participants

3

Reactant 2

HCID 6363IsopropylamineHCID 19926930HCID 19926930, compound

Product 1

HCID 19926931HCID 19926931, compoundYield 100.3%

Procedure

3-Acetyl-8-methyl-4-methylsulfoxy-2-quinolinone (2.63g, 0.01 mol) and isopropylamine (0.6g, 0.01 mol) were used, but the reaction was carded out as the above process of example 37 to obtain the desired product (2.59g, yield: 68%).

Sources & evidence

ORD record
ord-2e91a1059cca48268ed8f59d36bfadb9
Source dataset
uspto-grants-1995_07
Patent number
US05430153

Reaction notes

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