Ethylamine → HCID 19926915, compound

HRID 1647279Notes

Reaction equation

[C:1]([C:4]1[C:5](=[O:25])[NH:6][C:7]2[C:12]([C:13]=1C)=[C:11](OS(O)(=O)=O)[C:10]([Cl:20])=[CH:9][C:8]=2[C:21]([F:24])([F:23])[F:22])(=[O:3])[CH3:2].[CH2:26]([NH2:28])[CH3:27]>>[C:1]([C:4]1[C:5](=[O:25])[NH:6][C:7]2[C:12]([C:13]=1[NH:28][CH2:26][CH3:27])=[CH:11][C:10]([Cl:20])=[CH:9][C:8]=2[C:21]([F:24])([F:22])[F:23])(=[O:3])[CH3:2]

Participants

Reactant 2

HCID 6341Ethylamine

HCID 86748764HCID 86748764, compound

Product 1

HCID 19926915HCID 19926915, compoundYield 76%

Procedure

3-Acetyl-6-chloro-8-trifluoromethyl-4-methylsulfoxy-2-quinolinone (3.5g, 0.01 mol) and ethylamine(70 wt % solution; 0.65g, 0.01 mol) were used, but the reaction was carried out as the above process of example 37 to obtain the desired product (2.52g, yield: 76%).

Sources & evidence

ORD record: ord-25b26b98a31f41858ddbd13f1c37a74b
Source dataset: uspto-grants-1995_07
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US05430153

Reaction notes

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