Cyclopentylamine → HCID 19926929, compound

HRID 1647282Notes

Reaction equation

[C:1]([C:4]1[C:5](=[O:22])[NH:6][C:7]2[C:12]([C:13]=1C)=[C:11](OS(O)(=O)=O)[CH:10]=[CH:9][C:8]=2[CH2:20][CH3:21])(=[O:3])[CH3:2].[CH:23]1([NH2:28])[CH2:27][CH2:26][CH2:25][CH2:24]1>>[C:1]([C:4]1[C:5](=[O:22])[NH:6][C:7]2[C:12]([C:13]=1[NH:28][CH:23]1[CH2:27][CH2:26][CH2:25][CH2:24]1)=[CH:11][CH:10]=[CH:9][C:8]=2[CH2:20][CH3:21])(=[O:3])[CH3:2]

Participants

Reactant 2

HCID 2906Cyclopentylamine

HCID 19926870HCID 19926870, compound

Product 1

HCID 19926929HCID 19926929, compoundYield 72.1%

Procedure

3-Acetyl-8-ethyl-4-methylsulfoxy-2-quinolinone (2.77g, 0.01 mol) and cyclopentylamine (0.86g, 0.01 mol) were used, but the reaction was carried out as the above process of example 37 to obtain the desired product (2.15g, yield: 72%).

Sources & evidence

ORD record: ord-1713f88c75f549b5a99e159cb09a0e45
Source dataset: uspto-grants-1995_07
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US05430153

Reaction notes

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