Sec-Butylamine → HCID 19926928, compound

HRID 1647284Notes

Reaction equation

[C:1]([C:4]1[C:5](=[O:23])[NH:6][C:7]2[C:12]([C:13]=1C)=[C:11](OS(O)(=O)=O)[CH:10]=[CH:9][C:8]=2[CH:20]([CH3:22])[CH3:21])(=[O:3])[CH3:2].[CH:24]([NH2:28])([CH2:26][CH3:27])[CH3:25]>>[C:1]([C:4]1[C:5](=[O:23])[NH:6][C:7]2[C:12]([C:13]=1[NH:28][CH:24]([CH2:26][CH3:27])[CH3:25])=[CH:11][CH:10]=[CH:9][C:8]=2[CH:20]([CH3:21])[CH3:22])(=[O:3])[CH3:2]

Participants

Reactant 2

HCID 24874Sec-Butylamine

HCID 86748766HCID 86748766, compound

Product 1

HCID 19926928HCID 19926928, compoundYield 90%

Procedure

3-Acetyl-4-methylsulfoxy-8-isopropyl-2-quinolinone (2.91g, 0.01 mol) and sec-butylamine (0.73g, 0.01 mol) were used, but the reaction was carried out as the above process of example 37 to obtain the desired product (2.7g, yield: 90%).

Sources & evidence

ORD record: ord-aef618c194974b50b7a201857dc4510d
Source dataset: uspto-grants-1995_07
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US05430153

Reaction notes

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