HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Methyl-N-(3,4,5-trimethoxybenzyl)aniline → HCID 373805, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Methyl-N-(3,4,5-trimethoxybenzyl)aniline | HCID 373798 | — |
| Reactant | 151221-94-2 | HCID 373812 | — |
| Product | HCID 373805 | HCID 373805 | 90.2% |
Reaction Steps
From 108f (8.2 g, 26.0 mmol), a similar procedure as described for 109a gave 109f (7.4 g, 89.8%) as an oil. 1H NMR (200 MHz, CDCl3) δ7.06 (d, J=8 Hz, 2H), 6.61 (d, J=8 Hz, 2H), 6.61 (s, 2H), 4.24 (s, 2H), 3.84 (s, 9H), 2.81 (h, J=8 Hz, 1H, 1.21 (d, J=8 Hz, 6H). EIMS 315 (M+, 100).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05430062 |
| Source dataset | uspto-grants-1995_07 |
| ORD ID | ord-70df7c5917804bbd86ef37c6c0275c92 |
| Source note | uspto-grants-1995_07 |