HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Methoxy-N-(3,4,5-trimethoxybenzyl)aniline → 4-Methoxy-N-[(3,4,5-trimethoxyphenyl)methyl]aniline--hydrogen chloride (1/1)
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Methoxy-N-(3,4,5-trimethoxybenzyl)aniline | HCID 364716 | — |
| Reactant | 4-Methyl-N-[(3,4,5-trimethoxyphenyl)methyl]aniline--hydrogen chloride (1/1) | HCID 373799 | — |
| Product | 4-Methoxy-N-[(3,4,5-trimethoxyphenyl)methyl]aniline--hydrogen chloride (1/1) | HCID 372855 | 80.7% |
Reaction Steps
From 109c (9.0 g, 29.7 mmol), a similar procedure as described for 110a gave 110c (8.14 g, 80.7%) as tiny white crystals: mp 182°-4° C. 1H NMR (200 MHz, DMSO-d6) δ7.36 (d, J=8 Hz 2H), 6.98 (d, J=8 Hz, 2H), 6.62 (s, 2H), 4.36 (s, 2H), 3.74 (s, 9H), 3.63 (s, 3H). Anal. (C17H22ClNO4.1/2H2O)C, H, N.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05430062 |
| Source dataset | uspto-grants-1995_07 |
| ORD ID | ord-47f69964b363423ab14ffeefbc65895e |
| Source note | uspto-grants-1995_07 |