HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Methoxyaniline → HCID 178459173, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Methoxyaniline | HCID 7000 | — |
| Reactant | Methyl 2-(methoxymethylidene)-3-oxopentanoate | HCID 53662896 | — |
| Product | HCID 178459173 | HCID 178459173 | — |
Reaction Steps
A mixture of methyl 2-propanoyl-3-methoxyacrylate (70 g) and 2-methoxyaniline (45 ml) was heated on a steam bath for 30 minutes, then diluted with petroleum ether and left to crystallise. Filtration and washing with ether gave methyl 2-propanoyl-3-(2-methoxyphenylamino)acrylate (78.2 g) as a mixture of E/Z isomers.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05432182 |
| Source dataset | uspto-grants-1995_07 |
| ORD ID | ord-d0fd4ffff0174a3090b43fb5f7ab0982 |
| Source note | uspto-grants-1995_07 |