Methylamine → HCID 178482385, compound

Participants

Reaction Steps

2.9 g (0.093 mol) of gaseous methylamine were passed into a solution of 10 g (0.047 mol) of 2-amino-4-chlorodifluoromethoxy-6-fluoro-1,3,5-triazine in 150 ml of diethyl ether in the course of 20 minutes at 0° C. while stirring. Stirring was continued for one hour at 0° C. and overnight at 22° C. Washing with water, drying and evaporating down gave 9.4 g (89.5% of theory) of the title compound of melting point 143° C. (decomposition).

Provenance & Evidence