1-Chloro-4-nitrobenzene → HCID 10515564, compound

HRID 1647726Notes

Reaction equation

HRID 1647726 reaction equation
Cl[C:2]1[CH:7]=[CH:6][C:5]([N+:8]([O-:10])=[O:9])=[CH:4][CH:3]=1.[N:11]12[CH2:18][CH2:17][CH2:16][C:15]1([CH2:19][NH2:20])[CH2:14][CH2:13][CH2:12]2>>[N:11]12[CH2:18][CH2:17][CH2:16][C:15]1([CH2:19][NH:20][C:2]1[CH:7]=[CH:6][C:5]([N+:8]([O-:10])=[O:9])=[CH:4][CH:3]=1)[CH2:14][CH2:13][CH2:12]2

Participants

3

Reactant 2

HCID 74741-Chloro-4-nitrobenzeneHCID 10654304(Hexahydro-1H-pyrrolizin-7A-YL)methanamine

Product 1

HCID 10515564HCID 10515564, compoundYield 74.4%

Procedure

p-Chloronitrobenzene and (1-azabicyclo[3.3.0]octan-5-yl)methylamine were reacted in the same manner as in Example 1 to obtain the titled compound as an oil in a yield of 74.4 %.

Sources & evidence

ORD record
ord-d363632d96c6408196aeae7efd187e9e
Source dataset
uspto-grants-1995_07
Patent number
US05434165

Reaction notes

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