(Hexahydro-1H-pyrrolizin-7A-YL)methanamine → HCID 15296220, compound

HRID 1647733Notes

Reaction equation

HRID 1647733 reaction equation
Br[C:2]1[C:3]2[C:8]([C:9]([N+:16]([O-:18])=[O:17])=[C:10]3[C:15]=1[CH:14]=[CH:13][CH:12]=[CH:11]3)=[CH:7][CH:6]=[CH:5][CH:4]=2.[N:19]12[CH2:26][CH2:25][CH2:24][C:23]1([CH2:27][NH2:28])[CH2:22][CH2:21][CH2:20]2>>[N:19]12[CH2:26][CH2:25][CH2:24][C:23]1([CH2:27][NH:28][C:2]1[C:3]3[C:8]([C:9]([N+:16]([O-:18])=[O:17])=[C:10]4[C:15]=1[CH:14]=[CH:13][CH:12]=[CH:11]4)=[CH:7][CH:6]=[CH:5][CH:4]=3)[CH2:22][CH2:21][CH2:20]2

Participants

3

Reactant 2

HCID 10654304(Hexahydro-1H-pyrrolizin-7A-YL)methanamineHCID 130239799-Bromo-10-nitroanthracene

Product 1

HCID 15296220HCID 15296220, compoundYield 51.5%

Procedure

9-Bromo-10-nitroanthracene and (1-azabicyclo[3.3.0]octan-5-yl)methylamine were reacted in the same manner as in Example 1 to obtain the titled compound in a yield of 51.5%.

Sources & evidence

ORD record
ord-50ff8383c05040c5ae85b69c6bd8eed0
Source dataset
uspto-grants-1995_07
Patent number
US05434165

Reaction notes

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