HCID 67806829, compound → HCID 15225626, compound

HRID 1647871Notes

Reaction equation

HRID 1647871 reaction equation
Cl.[CH3:2][O:3][C:4]([CH2:6][CH2:7][NH:8][C:9](=[O:27])[C:10]1[CH:15]=[CH:14][C:13]([NH:16][CH2:17]CCN2CCSCC2)=[C:12]([NH2:26])[CH:11]=1)=[O:5]>C(OCC)(=O)C.C(O)C>[CH3:2][O:3][C:4]([CH2:6][CH2:7][NH:8][C:9](=[O:27])[C:10]1[CH:15]=[CH:14][C:13]([NH:16][CH3:17])=[C:12]([NH2:26])[CH:11]=1)=[O:5]

Participants

3

Reactant 1

HCID 67806829HCID 67806829, compound

Product 1

HCID 15225626HCID 15225626, compound

Reagents, catalysts & solvents 1

HCID 21584252Ethanol ethylacetateSolvent

Procedure

The same procedure is used as in (2). Rf value: 0.28 (silica gel; ethyl acetate/ethanol=50:2)

Sources & evidence

ORD record
ord-62d5a01b315e4f49836e1dd8273fdda2
Source dataset
uspto-grants-1995_07
Patent number
US05434150

Reaction notes

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