HCID 67806829, compound → HCID 67804861, compound

HRID 1647875Notes

Reaction equation

HRID 1647875 reaction equation
Cl.[CH3:2][O:3][C:4]([CH2:6][CH2:7][NH:8][C:9](=[O:27])[C:10]1[CH:15]=[CH:14][C:13]([NH:16][CH2:17][CH2:18][CH2:19]N2CCSCC2)=[C:12]([NH2:26])[CH:11]=1)=[O:5]>C(OCC)(=O)C.C(O)C>[CH3:2][O:3][C:4]([CH2:6][CH2:7][NH:8][C:9](=[O:27])[C:10]1[CH:15]=[CH:14][C:13]([NH:16][CH2:17][CH2:18][CH2:19][CH2:9][C:10]2[CH:15]=[CH:14][CH:13]=[CH:12][CH:11]=2)=[C:12]([NH2:26])[CH:11]=1)=[O:5]

Participants

3

Reactant 1

HCID 67806829HCID 67806829, compound

Product 1

HCID 67804861HCID 67804861, compound

Reagents, catalysts & solvents 1

HCID 21584252Ethanol ethylacetateSolvent

Procedure

The same procedure is used as in (2). Rf value: 0.68 (silica gel; ethyl acetate/ethanol=9:1)

Sources & evidence

ORD record
ord-c3488c4ba0ee4b84a9188696770b378e
Source dataset
uspto-grants-1995_07
Patent number
US05434150

Reaction notes

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