Ethanol ethylacetate → HCID 67804708, compound

HRID 1647879Notes

Reaction equation

Cl.[CH3:2][O:3][C:4]([CH2:6][CH2:7][NH:8][C:9](=[O:29])[C:10]1[CH:15]=[CH:14][C:13]([NH:16][CH2:17][CH2:18][CH2:19]N2CCSCC2)=[C:12]([N+:26]([O-:28])=[O:27])[CH:11]=1)=[O:5].C(O[CH2:34][CH3:35])(=O)C.[CH2:36](O)[CH3:37]>>[CH3:2][O:3][C:4]([CH2:6][CH2:7][NH:8][C:9](=[O:29])[C:10]1[CH:15]=[CH:14][C:13]([NH:16][CH2:17][CH2:18][CH2:19][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:36][CH2:37][CH2:34][CH3:35])=[C:12]([N+:26]([O-:28])=[O:27])[CH:11]=1)=[O:5]

Participants

Reactant 2

HCID 21584252Ethanol ethylacetate

HCID 67806095HCID 67806095, compound

Product 1

HCID 67804708HCID 67804708, compound

Procedure

The same procedure is used as in (1). Rf value: 0.78 (silica gel; ethyl acetate/ethanol=50:2)

Sources & evidence

ORD record: ord-9a128028e6cb4bfcb68e0be6f547df69
Source dataset: uspto-grants-1995_07
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US05434150

Reaction notes

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