HCID 67806095, compound → HCID 67806005, compound

HRID 1647880Notes

Reaction equation

HRID 1647880 reaction equation
Cl.[CH3:2][O:3][C:4]([CH2:6][CH2:7][NH:8][C:9](=[O:29])[C:10]1[CH:15]=[CH:14][C:13](NCCCN2CCSCC2)=[C:12]([N+:26]([O-])=O)[CH:11]=1)=[O:5]>C(Cl)Cl.CO>[CH3:2][O:3][C:4]([CH2:6][CH2:7][NH:8][C:9](=[O:29])[C:10]1[CH:15]=[CH:14][CH:13]=[C:12]([NH2:26])[C:11]=1[NH:8][CH2:9][C:10]1[CH:15]=[CH:14][CH:13]=[CH:12][CH:11]=1)=[O:5]

Participants

3

Reactant 1

HCID 67806095HCID 67806095, compound

Product 1

HCID 67806005HCID 67806005, compound

Reagents, catalysts & solvents 1

HCID 21226129Dichloromethane methanolSolvent

Procedure

The same procedure is used as in (1). Rf value: 0.69 (silica gel; methylene chloride/methanol=9:1)

Sources & evidence

ORD record
ord-5856269fe5224bbe84227052abe5a7fc
Source dataset
uspto-grants-1995_07
Patent number
US05434150

Reaction notes

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