HCID 67806095, compound → HCID 67804809, compound

HRID 1647881Notes

Reaction equation

HRID 1647881 reaction equation
Cl.[CH3:2][O:3][C:4]([CH2:6][CH2:7][NH:8][C:9](=[O:29])[C:10]1[CH:15]=[CH:14][C:13]([NH:16][CH2:17][CH2:18][CH2:19]N2CCSCC2)=[C:12]([N+:26]([O-:28])=[O:27])[CH:11]=1)=[O:5]>C(Cl)Cl.CO>[CH3:2][O:3][C:4]([CH2:6][CH2:7][NH:8][C:9](=[O:29])[C:10]1[CH:15]=[CH:14][C:13]([NH:16][CH2:17][CH2:18][CH2:19][CH2:9][C:10]2[CH:15]=[CH:14][CH:13]=[CH:12][CH:11]=2)=[C:12]([N+:26]([O-:28])=[O:27])[CH:11]=1)=[O:5]

Participants

3

Reactant 1

HCID 67806095HCID 67806095, compound

Product 1

HCID 67804809HCID 67804809, compound

Reagents, catalysts & solvents 1

HCID 21226129Dichloromethane methanolSolvent

Procedure

The same procedure is used as in (1). Rf value: 0.51 (silica gel; methylene chloride/methanol=19:1)

Sources & evidence

ORD record
ord-6f47a6c42b1d4e4cafae6fe0ab032475
Source dataset
uspto-grants-1995_07
Patent number
US05434150

Reaction notes

Loading…