Ethanol ethylacetate → HCID 19921161, compound

HRID 1647882Notes

Reaction equation

Cl.CO[C:4]([CH2:6][CH2:7][NH:8][C:9](=[O:29])[C:10]1[CH:15]=[CH:14][C:13]([NH:16][CH2:17]CCN2CCSCC2)=[C:12]([N+:26]([O-:28])=[O:27])[CH:11]=1)=O.[C:30]([O:33][CH2:34]C)(=[O:32])[CH3:31].C(O)C>>[CH3:34][O:33][C:30]([CH:31]1[CH2:4][CH2:6][CH2:7][N:8]1[C:9](=[O:29])[C:10]1[CH:15]=[CH:14][C:13]([NH:16][CH3:17])=[C:12]([N+:26]([O-:28])=[O:27])[CH:11]=1)=[O:32]

Participants

Reactant 2

HCID 21584252Ethanol ethylacetate

HCID 67806095HCID 67806095, compound

Product 1

HCID 19921161HCID 19921161, compound

Procedure

The same procedure is used as in (1). Rf value: 0.57 (silica gel; ethyl acetate/ethanol=9:1)

Sources & evidence

ORD record: ord-d7e1fe14b0e24acfae134772b7ba5e00
Source dataset: uspto-grants-1995_07
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US05434150

Reaction notes

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